Papers › Hypothesis Learning in Automated Experiment: Application to Combinatorial Materials Libraries

Hypothesis Learning in Automated Experiment: Application to Combinatorial Materials Libraries

13 Dec 2021arXiv:2112.06649links table onlyarchive 2025-07-28

Maxim Ziatdinov, Yongtao Liu, Anna N. Morozovska, Eugene A. Eliseev, Xiaohang Zhang, Ichiro Takeuchi, Sergei V. Kalinin

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Machine learning is rapidly becoming an integral part of experimental physical discovery via automated and high-throughput synthesis, and active experiments in scattering and electron/probe microscopy. This, in turn, necessitates the development of active learning methods capable of exploring relevant parameter spaces with the smallest number of steps. Here we introduce an active learning approach based on co-navigation of the hypothesis and experimental spaces. This is realized by combining the structured Gaussian Processes containing probabilistic models of the possible system's behaviors (hypotheses) with reinforcement learning policy refinement (discovery). This approach closely resembles classical human-driven physical discovery, when several alternative hypotheses realized via models with adjustable parameters are tested during an experiment. We demonstrate this approach for exploring concentration-induced phase transitions in combinatorial libraries of Sm-doped BiFeO3 using Piezoresponse Force Microscopy, but it is straightforward to extend it to higher-dimensional parameter spaces and more complex physical problems once the experimental workflow and hypothesis-generation are available.

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